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Tuesday, May 12, 2020 | History

2 edition of High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk found in the catalog.

High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk

Komoroski

High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk

by Komoroski

  • 131 Want to read
  • 11 Currently reading

Published by John Wiley & Sons Inc .
Written in

    Subjects:
  • Chemistry

  • The Physical Object
    FormatHardcover
    Number of Pages380
    ID Numbers
    Open LibraryOL10303746M
    ISBN 100471186708
    ISBN 109780471186700

    Text Books: Understanding NMR Spectroscopy, James Keeler, John Wiley & Sons. ISBN High Resolution NMR Techniques in Organic Chemistry (Second Edition), T.D.W. Claridge, Tetrahedron Organic Chemistry, Vol Elsevier. ISBNFile Size: 1MB. Where a substance in the solid state is concerned, high‐resolution 13 C‐NMR spectroscopy provides not only information about the chemical structure, but also about the solid state itself. To mention just a few examples, information on the conformation, crystal structure and molecular dynamics, as well as molecular miscibility is given.

    Polymer Applications of Solid-State NMR Polymers Above T g: Elastomers and Melts High-resolution MAS MQ NMR on elastomers and melts Polymers Around and Below T g Conformations of polymers in the glassy state   Nuclear magnetic resonance (NMR) spectroscopy is a premiere technique for the studies of polymers. It is widely used for polymer identification, quality control, and reaction monitoring to structure determination, polymer morphology, compatibility, chain .

    High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk by R. A. Komoroski A copy that has been read, but remains in clean condition. All pages are intact, and the cover is intact. The spine may show signs of wear. Pages can include limited notes and highlighting, and the copy can include previous owner inscriptions. • Can use 13C-NMR to detect and quantify these different types of branching • This technique is based upon the chemical shifts of the carbon atoms on the backbone chain attached to the branch. • The chemical shift depends on the length of the branch for branches up to 6 carbons in length. It is the same for all branches 6 carbons and longer.


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High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk by Komoroski Download PDF EPUB FB2

This book is an authoritative and comprehensive account of the principles and practice of modern NMR spectroscopy of solid polymers to determine their structure and dynamics at a molecular level.

Book Review: High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk. Edited by R. KomoroskiAuthor: Hans Wolfgang Spiess. The various techniques used to analyze the microstructures of polymers are presented in this book. High resolution and solid state techniques are described, and applications to both synthetic and biological polymers are discussed in detail.

Particular emphasis is placed on the determination of polymer microstructure by NMR by: Book Review: High resolution NMR spectroscopy of synthetic polymers in bulk.

edited by Richard A. Komoroski, VCH Publishers, Deerfield Beach, FL,pp.price DM A practical guide to the study and understanding of the structure of synthetic polymer materials using the complete range of microscopic techniques. The major part of the book is devoted to specimen preparation and applications.

New applications and additional references provide a critical update. Category: Technology & Engineering. About this book. This book provides a source of information on all major aspects of NMR spectroscopy of synthetic polymers. It represents a deliberate attempt to pull together the numerous strands of the subject in a single comprehensive volume, designed to be readable at every scientific level.

This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.

This book is a valuable resource for chemists and research workers. High Resolution NMR of Macromolecules presents the development in the NMR study of polymers.

This book discusses the exciting area of application of NMR to polymer science as the result of the more general accessibility of instruments of high magnetic field. Vulcanized rubbers, i.e., vulcanized natural rubber and vulcanized chloroprene rubber, were characterized by rubber-state NMR resolution 1 H and 13 C-NMR spectra were accomplished for the vulcanized rubbers due to fast magic angle spinning.

The correlation between 1 H and 13 C of the vulcanized rubbers was investigated by one- and two-dimensional : Seiichi Kawahara, Yoshimasa Yamamoto, Takayuki Saito.

Abstract. High resolution nuclear magnetic resonance (HR-NMR) spectroscopy is the apellative given to the measurement of NMR spectra under conditions that enable magnetically nonequivalent nuclei of the same spin species (e.g., protons or carbon) to be resolved as individual resonance by: Description.

High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences. It is written at an "intermediate". Description High Resolution NMR of Macromolecules presents the development in the NMR study of polymers.

This book discusses the exciting area of application of NMR to polymer science as the result of the more general accessibility of instruments of high magnetic Edition: 1.

Reviews the principles and application of high resolution NMR in polymers. Triplet Exciton Generation in Bulk-Heterojunction Solar Cells Based on Endohedral Fullerenes. Polymer Molecular Weight Analysis by 1H NMR Spectroscopy.

Journal of Chemical Education88 (8), DOI: /edv. Cited by: 5. "NMR Spectroscopy of Polymers covers in detail all aspects of the NMR spectroscopic analysis of polymers.

this is an excellent reference book for synthetic polymer chemists and contains many useful practical points in addition to providing detailed coverage of the theoretical aspects of NMR spectroscopy.". Overview of NMR of Bulk Polymers Hans Wolfgang Spiess Chapter 2, DOI: /bkch Publication Date (Web): Octo Komoroski RA (ed) () High resolution NMR spectroscopy of Synthetic Polymers in Bulk.

VCH, New York Google Scholar Wind RA, Dec SF, Lock H, Maciel GE () J. Cited by: 1. Natural and Synthetic High Polymers: Lectures Presented at the Seventh Colloquium on N.M.R. Spectroscopy (NMR Basic Principles and Progress (4)) [Kosfeld, R.] on *FREE* shipping on qualifying offers.

Natural and Synthetic High Polymers: Lectures Presented at the Seventh Colloquium on N.M.R. Spectroscopy (NMR Basic Principles and Progress (4))Format: Paperback. Experimental practice in high-resolution solution-state NMR of polymers 16 The spectrometer 16 The sample 17 Advanced Fourier transform techniques 18 One-dimensional techniques 19 Two-dimensional NMR spectroscopy 22 A survey of applications of high-resolution solution-state NMR to polymers trends in analytical chemistry, aol.

2, no. 3, Proton and carbon high resolution NMR spectroscopy of high polymers Using a super-conducting magnet, the examination of high polymers by 1H- and 13C-NMR provides complementary and precise information about their by: 3.

Proton and Carbon NMR Spectra of Polymers. Quang Tho Pham. Taylor & Francis, - Carbon - pages. 1 Review. Contains NMR spectra with associated analytical notes covering acrylics, 4/5(1).

ISBN: OCLC Number: Description: xi, pages: illustrations ; 25 cm. Contents: Overview of High-Resolution NMR of Solid Polymers; Principles and General Aspects of High-Resolution NMR of Bulk Polymers; High-Resolution NMR of Glassy Amorphous Polymers; Carbon NMR of Solid Amorphous Polymers Above Tg; Carbon Solid-State NMR .“NMR Spectroscopy of Polymers” Tutorial.

ACS National Meeting. New Orleans, April 6, Overview of NMR of Bulk Polymers. Overview of NMR of Bulk Polymers.Proton NMR spectroscopy of solids has traditionally been challenging due to the widespread presence of strong ¹H-¹H dipolar couplings in solid systems, which severely broaden proton NMR spectral.